Please use this identifier to cite or link to this item: http://repositorio.inesctec.pt/handle/123456789/7215
Title: Automatized and desktop AC-susceptometer for the in situ and real time monitoring of magnetic nanoparticles' synthesis by coprecipitation
Authors: Fernandez Garcia,MP
Teixeira,JM
Machado,P
Mariana Rafaela Oliveira
João Miguel Maia
Pereira,C
Pereira,AM
Freire,C
Araujo,JP
Issue Date: 2015
Abstract: The main purpose of this work was to design, develop, and construct a simple desktop AC susceptometer to monitor in situ and in real time the coprecipitation synthesis of magnetic nanoparticles. The design incorporates one pair of identical pick-up sensing coils and one pair of Helmholtz coils. The picked up signal is detected by a lock-in SR850 amplifier that measures the in-and out-of-phase signals. The apparatus also includes a stirrer with 45 degrees-angle blades to promote the fast homogenization of the reaction mixture. Our susceptometer has been successfully used to monitor the coprecipitation reaction for the synthesis of iron oxide nanoparticles. (C) 2015 AIP Publishing LLC.
URI: http://repositorio.inesctec.pt/handle/123456789/7215
http://dx.doi.org/10.1063/1.4918723
metadata.dc.type: article
Publication
Appears in Collections:LIAAD - Articles in International Journals

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